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Equipment used for these procedures includes the instruments described above (Perkin Elmer 2400 Series II CHN Analyzer and a UIC Coulometrics Coulometer with an Acidification Unit), as well as a ball-mill grinder used to grind the dried sediment …

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The 3C-SiC nanopowder obtained by dry grinding of the formed free nanoporous layer (see Section 11.2) was directly dispersed in a Krebs buffer solution.The formed suspension was centrifuged at 5,000g for 3 min in order to sediment out large crystallites at the bottom of the centrifuge vials and to collect the useful top part of the suspension containing only very small (<10 nm) and uniformly ...

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Place grinding vessel in the ball mill grinder and screw tightly to hold the vessel in place. Start the machine by closing the door of the ball mill grinder. While the sample is being ground, use compressed air to remove excess sediment left in the original sample …

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A 22-liters laboratory grinding ball mill was used; its drum diameter (D) and length (L) were 300 and 300 mm, respectively. The mill operated at 75% of the critical rotational speed (N c = 42.3 / D), which corresponded to 75 rpm. A total of 40 kg stainless steel balls (20 kg of 15-mm diameter and 20 kg of 5-mm diameter) were employed.

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SEDIMENT GRINDING PROCEDURE - USGS

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